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Assignment of the Absolute Configuration of Polyfunctional Compounds

Josi M. Seco, Emilio Quiqoa, and Ricardo Riguera

in The Assignment of the Absolute Configuration by NMR using Chiral Derivatizing Agents: A Practical Guide

Published in print:
2015
Published Online:
November 2020
ISBN:
9780199996803
eISBN:
9780197563373
Item type:
chapter
Publisher:
Oxford University Press
DOI:
10.1093/oso/9780199996803.003.0008
Subject:
Chemistry, Organic Chemistry

From a practical point of view, the assignment of the absolute configuration of sec/sec 1,2- and 1,n-diols does not require the separate derivatization (two different steps with the CDA of choice) ... More


Assignment of the Absolute Configuration of Monofunctional Compounds by Double Derivatization

Josi M. Seco, Emilio Quiqoa, and Ricardo Riguera

in The Assignment of the Absolute Configuration by NMR using Chiral Derivatizing Agents: A Practical Guide

Published in print:
2015
Published Online:
November 2020
ISBN:
9780199996803
eISBN:
9780197563373
Item type:
chapter
Publisher:
Oxford University Press
DOI:
10.1093/oso/9780199996803.003.0006
Subject:
Chemistry, Organic Chemistry

The assignment of secondary alcohols can be carried out by using one of several CDAs [13–15]. The most used and most reliable ones are MPA, 9-AMA, and MTPA [35–40]. Figure 3.1 shows their ... More


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