Naomi E. Chayen, John R. Helliwell, and Edward H. Snell
- Published in print:
- 2010
- Published Online:
- May 2010
- ISBN:
- 9780199213252
- eISBN:
- 9780191707575
- Item type:
- chapter
- Publisher:
- Oxford University Press
- DOI:
- 10.1093/acprof:oso/9780199213252.003.0015
- Subject:
- Physics, Crystallography: Physics
Unusual diffraction geometries may seem a curiosity but may stimulate novel avenues of application. Not least they illustrate a diversity of diffraction‐measuring possibilities. Laue diffraction ...
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Unusual diffraction geometries may seem a curiosity but may stimulate novel avenues of application. Not least they illustrate a diversity of diffraction‐measuring possibilities. Laue diffraction including 3‐dimensional detector arrangements is described. The particular congestion of neutron Laue diffraction patterns with big crystals is highlighted. The large‐angle oscillation technique is discussed including the principle with the Ewald sphere construction and practical examples of ‘LOT’ diffraction patterns. Ultra‐fine‐phi‐slicing with perfect or near‐perfect crystals is described. Particular success has been obtained with Laue diffraction where applications to time‐resolved structural intermediates using synchrotron radiation as well as hydrogen and hydration in macromolecular structure are described.Less
Unusual diffraction geometries may seem a curiosity but may stimulate novel avenues of application. Not least they illustrate a diversity of diffraction‐measuring possibilities. Laue diffraction including 3‐dimensional detector arrangements is described. The particular congestion of neutron Laue diffraction patterns with big crystals is highlighted. The large‐angle oscillation technique is discussed including the principle with the Ewald sphere construction and practical examples of ‘LOT’ diffraction patterns. Ultra‐fine‐phi‐slicing with perfect or near‐perfect crystals is described. Particular success has been obtained with Laue diffraction where applications to time‐resolved structural intermediates using synchrotron radiation as well as hydrogen and hydration in macromolecular structure are described.
